[ Identification | Description | Input parameters | Links ]
ILL_D2B_noenv
InstrumentThe diffractometer D2B is characterised by the very high take-off angle (135 deg) for the monochromator, which has a relatively large mosaic spread of 20' to compensate for the corresponding intensity (dl/l) loss. It is 300 mm high, focusing vertically onto about 50 mm; this large incident vertical divergence is matched by 200 mm high detectors and collimators. A complete diffraction pattern is obtained after about 100 steps of 0.025 deg in 2theta, since the 64 detectors are spaced at 2.5 deg intervals. Such scans take typically 30 minutes; they are repeated to improve statistics. D2B was designed for work on samples and high resolution of very large d-spacings using wavelengths of between 2.4 Å and 6 Å. Wavelengths can easily be changed under computer control, since they are all obtained by a simple rotation within the Ge[hhl] plane. A large graphite filter can be switched in to provide a very clean beam at 2.4 Angs, and a cold Be-filter can be used for longer wavelengths. This model implements as well the Caglioti UVW equations, that give estimates of the instrument resolution. Monochromator lattice parameter Ge 111 DM=3.266 AA Ge 311 DM=1.714 AA Ge 511 DM=1.089 AA Ge 533 DM=0.863 AA
Name | Unit | Description | Default |
lambda | Angs | Wavelength at monochromator, computed from DM and THETA_M if left as 0. | 1.594 |
DM | Angs | d-spacing of monochromator, computed from lambda and THETA_M if left as 0. | 0 |
Powder | str | File name for powder description | "Na2Ca3Al2F14.laz" |
RV | m | Monochromator vertical curvature, 0 for flat, -1 for automatic setting | -1 |
L1 | m | Source-Monochromator distance | 16.05 |
L2 | m | Monochromator-Sample distance | 2.645 |
L3 | m | Sample-Detector distance | 1.3 |
verbose | 1 | Print DIF configuration. 0 to be quiet | 1 |
ALPHA1 | min | Horizontal collimator divergence for L1 arm (before monochromator) | 18 |
ALPHA2 | min | Horizontal collimator divergence for L2 arm (monochromator-sample) | 11 |
ALPHA3 | min | Horizontal collimator divergence for L3 arm (sample-detector) | 5 |
ETA | min | Monochromator horizontal mosaic (gaussian) | 12 |
THETA_M | deg | Monochromator take-off angle, computed from lambda and DM if left as 0. | 67.5 |
TILT | deg | Monochromator additional tilt, for rocking curves | 0 |
SM | 1 | Scattering sense of beam from Monochromator. 1:left, -1:right | 1 |
Dheight | m | Banana detector height | 0.3 |
coating | 1 | Super-mirror in-beam tube guide coating | 0 |
ILL_D2B_noenv.instr
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[ Identification | Description | Input parameters | Links ]
Generated on 2023-09-19 20:01:36